Noble Liquid Test Facility (NLTF)

The main liquid argon testing facility, the Noble Liquid Test Facility, is located at the Proton Assembly Building and consists of four liquid argon cryostats, three of which can be booked for general R&D tests. It also offers working areas for smaller temporary setups, including several open dewars. The four test stands are:

  • Luke, also known as the Material Test Stand, mainly used to study the impact of materials on the electron lifetime.
  • TallBo, mainly used for developing scintillation light collection technologies.
  • Blanche, multipurpose cryostat mainly used for studying high voltage breakdown in noble liquids and/or small to medium size experimental setups.
  • Iceberg, a 3000L cryostat, mainly used for DUNE related tests.

Please contact the facility coordinator (Flor de Maria Blaszczyk) if you have any questions about the facility, how to become a user, and what procedures need to be followed to make a request. Please make sure you contact the facility manager before submitting a TSW to make sure the facility does meet your needs. Requests for time on any of these test stands may be made following these instructions.


How to get to the NLTF

The NLTF is located inside the the Proton Assembly Building also known as PAB. See map below.

NLTF services and equipment

The NLTF is the home of Luke (also known as the Material Test Stand), Tall Bo, Blanche, and Iceberg. All permanent setups at PAB have access to a suite of gas analyzers which can detect oxygen and water concentrations at the parts-per-billion (ppb) level, and nitrogen concentrations at the parts-per-million level. The liquid argon delivery system at PAB includes single-pass inline filtration to further remove water and oxygen from the argon before it enters the different test stands. The liquid argon delivered to the different cryostats is considered ultra-pure. The typical oxygen level after filtration is less than 1 ppb, and the water concentration is a few ppb. Nitrogen levels vary, depending directly on what the vendor can deliver but stay typically below 1 ppm.

With the exception of Tall Bo, all cryostats are equipped with a purity monitor which measures the electron lifetime in real time.

Luke / Material Test Stand (MTS)

The Materials Test Stand (MTS) is used for vetting materials that could potentially go into a liquid argon TPC experiment. The test stand has an argon lock through which one may access a sample cage. The argon delivered into the cryostat has been filtered for oxygen and water contamination and is ultra pure. The MTS has its own filter for removing any oxygen or water introduced with a sample. It also has a nitrogen cooled condensor to allow closed operation without boiling off the argon. There is a purity monitor inside the cryostat for monitoring the effect of any material on the electron lifetime of the liquid argon.

The sample size for testing is limited to the size of the opening for placing the sample into the basket used to convey the sample through the vapor and liquid space. The opening is 3.75 inches by 4.75 inches and the basket is cylindrical with a 5.5 inch diameter and 10 inch height. Very small samples can be tested by placing them into a perforated stainless steel box

The sample will be cleaned based on the user’s preferences. The cleaning methods can include any combination of no cleaning; wiping the sample with alcohol; ultrasonic cleaning with alcohol; baking the sample in air; evacuating the sample at room temperature; evacuating the sample at an elevated temperature.

The airlock is evacuated before any samples are inserted into the basket. Once the sample is inserted, it can be purged with argon gas or evacuated based on the user preference.

Three tests are possible with this system. The first is a room temperature test where the sample stays in the airlock and the valve to the cryostat is opened. During this test the internal liquid argon filter is turned off. This test can last from one to several days based on user preference. After a room temperature test the valve to the cryostat is closed and the internal filter is activated to clean up the liquid argon. The second test is a liquid test where the sample is lowered into the liquid and the internal filter is turned off. This test can last one to several days based on the user preference. The final test is the vapor test where the sample is placed in the vapor space at a temperature between 120-220K. Again, this test can last one to several days based on the user preference. For all the tests the electron drift lifetime is measured and the water level is monitored in the vapor. The results of the tests and pictures of the sample will be stored in the sample database on DocDB.

If you wish to test materials in the MTS please send an email specifying the material to be tested and which experiment or project the test supports. Please also specify how the material is to be prepared and the tests to be performed.

Please do not send materials without first contacting the facility using the email address linked above.

TallBo

TallBo is a cylindrical cryostat primarily used for developing scintillation light collection technologies for LArTPC detectors. It has a 56 cm inner diameter and up to a 183 cm liquid depth for a total volume of liquid argon of 451 liters. The cryostat is vacuum-jacketed for insulating the liquid argon. The drawings for TallBo are available on the LArTPC Doc-DB. The argon used to fill TallBo is filtered to remove oxygen and water contamination. TallBo has a nitrogen cooled condensor in order to provide a closed system without boil-off of the liquid argon.

A vertical mover is available for use in TallBo. It is 6 feet in length and consists of a slotted channel and screw capable of moving an object mounted on the screw up and down. Outside of TallBo the mover is controlled by a rotating wheel. A counter is attached to the wheel to keep track of the position. A “Lazy Susan” device is available for installation in TallBo as well. The device is attached to a rotating 6 foot long tube and has two 3.5 inch disks that can be spaced up to 54 inches apart. These disks have the capability to mount up to 12 devices on them. The disks can be easily detached to be replaced with custom mounts. The device is controlled with a rotating wheel outside the cryostat.

Although TallBo has primarily served as a light collection test facility, one could also test other kinds of systems in TallBo such as electronics and small TPCs.

Blanche

Blanche is a cylindrical cryostat primarily used for understanding issues related to high voltage breakdown in liquid argon. It is 152 cm tall with a 76 cm inner diameter; in practice, it is only filled to a depth of 122 cm for a total volume of liquid argon of 556 liters. The cryostat is vacuum-jacketed for insulating the liquid argon. The drawings for Blanche are available on the LArTPC Doc-DB. The argon used to fill Blanche is filtered to remove oxygen and water contamination. Blanche has a nitrogen cooled condensor in order to provide a closed system without boil-off of the liquid argon. Although Blanche has primarily served as a high voltage test facility, one could also test other kinds of systems in Blanche such as electronics and small TPCs.